HCID 15557329, compound → HCID 68148648, compound

HRID 267783Notes

Reaction equation

HRID 267783 reaction equation
O[C:2]1(CNC(C)C)COC2C=CC(O)=CC=2OC1.[CH:19]([N:22]1[CH2:26][C:25]2([CH2:32][O:31][C:30]3[CH:33]=[CH:34][C:35]([OH:37])=[CH:36][C:29]=3[O:28][CH2:27]2)[O:24][C:23]1=[O:38])([CH3:21])[CH3:20]>>[CH:19]([N:22]1[CH2:26][C:25]2([CH2:32][O:31][C:30]3[CH:33]=[CH:34][C:35]([O:37][CH3:2])=[CH:36][C:29]=3[O:28][CH2:27]2)[O:24][C:23]1=[O:38])([CH3:21])[CH3:20]

Participants

3

Reactant 2

HCID 15557329HCID 15557329, compoundHCID 15557332HCID 15557332, compound

Product 1

HCID 68148648HCID 68148648, compound

Procedure

This compound is prepared by employing the same reactants, reaction conditions and procedure outlined in Example 90 except the 3,7-dihydroxy-3-isopropylaminomethyl-3,4-dihydro-2H-1,5-benzodioxepin is replaced by an equivalent quantity of 3'-isopropyl-7-hydroxy-3,4-dihydro-2H-1,5-benzodioxepin-3-spiro-5'-oxazolidin-2'-one from Example 94, Step A.

Workup

  1. customThis compound is prepared
  2. customthe same reactants, reaction conditions and procedure

Sources & evidence

ORD record
ord-0ce4ecf07a88487fad97fe965311fc5f
Source dataset
uspto-grants-1976_03
Patent number
US03944560

Reaction notes

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