HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 4319207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3,4-Difluoroaniline | HCID 77469 | — |
| Reactant | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 4319207 | HCID 4319207 | — |
Reaction Steps
Subject 2.29 g. of adamantane carboxylic acid chloride (11.5 mmoles) 1.29 g. of (10 mmoles) 3,4-difluoro-aniline and 4.0 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from ethyl ether to yield the title product, m.p. 168.5°-170°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03944675 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-3e81be87136b4842a49626811fcee807 |
| Source note | uspto-grants-1976_03 |