HuagongsheHuagongshe Chemistry Print Report · For research reference only
Laurolactam → Octahydro-2H-azonin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Laurolactam | HCID 13690 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Product | Octahydro-2H-azonin-2-one | HCID 13632 | — |
Reaction Steps
0.3 mol % of sodium hydride and 0.3 mol % of the co-catalyst according to the Example 15 were dissolved in molten laurolactam. After 120 minutes at 160°C the polymerizate contained almost the equilibrium amount of the polyamide. Similar result was obtained with caprylolactam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03945984 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-986b257e956943cb868b45edf6eed37a |
| Source note | uspto-grants-1976_03 |