2-Chlorophenoxazine → 2-Chloro-10-[1-(1-pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine hydrochloride

HRID 267920노트

반응식

HRID 267920 반응식
[Cl:1][C:2]1[CH:15]=[CH:14][C:13]2[O:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[NH:5][C:4]=2[CH:3]=1.Cl.Cl[C:18]1[N:19]([C:23]2[CH2:27][CH2:26][CH2:25][N:24]=2)[CH2:20][CH2:21][CH:22]=1>>[ClH:1].[Cl:1][C:2]1[CH:15]=[CH:14][C:13]2[O:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[N:5]([C:18]3[N:19]([C:23]4[CH2:27][CH2:26][CH2:25][N:24]=4)[CH2:20][CH2:21][CH:22]=3)[C:4]=2[CH:3]=1

참가 물질

3

반응물 2

HCID 106325802-ChlorophenoxazineHCID 203071382-Chloro-1-(1-pyrrolin-2-yl) 2-pyrroline hydrochloride

생성물 1

HCID 203071342-Chloro-10-[1-(1-pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine hydrochloride

실험 절차

Reaction of 2-chlorophenoxazine with 2-chloro-(1-pyrrolin-2-yl)pyrroline hydrochloride according to the procedure of Example 7 affords 2-CHLORO-10-[1-(1-PYRROLIN-2-YL)-2-PYRROLIN-2-YL]-PHENOXAZINE HYDROCHLORIDE, m.p. 262.5°-264.5° C. (dec.) (corr.), from ethanol-ether.

출처 및 근거

ORD 기록
ord-9438839a2eee4778b67e033ad3eabb78
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03946004

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