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HRID267961

反应详情

EQUATION

反应方程式

HRID 267961 的结构方程式

REACTANTS

反应物

2
结构：ClCCN1CCCCC1
HCID74827

Piperidine, 1-(2-chloroethyl)-

C7H14ClN

结构：COc1ccc2c3c(c(=O)oc2c1OC)CNCC3
HCID13136911

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c3c(c(=O)oc2c1OC)CN(CCN1CCCCC1)CC3
HCID21508882

未命名化合物

PROCEDURE

实验过程

In the same way as described in Example 5, 5.7 mmoles of 1,2,3,4-tetrahydro-7,8-dimethoxy-5H-[1]benzopyrano[3,4-c]pryidin-5-one was alkylated with N-(2-chloroethyl)-piperidine to give, after recrystallization from MeOH, 0.5 g of product; mp 236°-239° C.

WORKUP

后处理

  1. customto give
  2. customafter recrystallization from MeOH, 0.5 g of product