HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 21495122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | 1-Bromo-2-[(chloromethyl)sulfanyl]benzene | HCID 21828494 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 21495122 | HCID 21495122 | 81.5% |
Reaction Steps
To a solution of 14.1 g of 2-aminopyridine in 180 ml of xylene is added a solution of 24.0 g of o-bromophenyl chloromethyl sulfide in 40 ml of xylene. The mixture is heated at 90°-95° for about fifteen hours to give about 27.3 g of the named compound, mp about 199°-201°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946025 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-eca9c38d06d543cf9dc72fa177bfb35b |
| Source note | uspto-grants-1976_03 |