Hydrochloric Acid → HCID 53698770, compound

Participants

Reaction Conditions

Reaction Steps

To a stirred suspension of 3-chloro-7-ethoxycarbonylmethoxyimino-7H-indolizino[5,6,7-ij]isoquinoline (0.356 g.) in ethanol (15 cc.) there is added N sodium hydroxide solution (1 cc.) followed by distilled water (35 cc.). After stirring for 1 hour at a temperature of about 20° C., a dark green solution is obtained which is neutralised by adding N hydrochloric acid (1 cc.). The resulting precipitate is filtered off, washed copiously with water and dried under reduced pressure. 3-Chloro-7-carboxymethoxyimino-7H-indolizino[5,6,7-ij]isoquinoline (0.28 g.), melting at 202° C. with decomposition, is thus obtained.

Provenance & Evidence