HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl oxalacetate → HCID 68136024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl oxalacetate | HCID 66951 | — |
| Reactant | 3-Fluorobenzaldehyde | HCID 68009 | — |
| Reactant | 2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- | HCID 643756 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68136024 | HCID 68136024 | — |
Reaction Steps
6.2 g of 3-fluorobenzaldehyde, 6.5 g of β-aminocrotonic acid ethyl ester and 9.5 g of oxalacetic acid diethyl ester in 40 ccs of ethanol are heated to the boil overnight, the mixture is evaporated in vacuo and a light yellow oil is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946028 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-77d9667d803a43729d68d433b1ef9e94 |
| Source note | uspto-grants-1976_03 |