HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl oxalacetate → HCID 86733114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl oxalacetate | HCID 66951 | — |
| Reactant | 2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- | HCID 643756 | — |
| Reactant | 2-azidobenzaldehyde | HCID 10888060 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86733114 | HCID 86733114 | — |
Reaction Steps
A solution of 14.7 g of 2-azidobenzaldehyde, 19 g of oxalacetic acid diethyl ester and 13 g of β-aminocrotonic acid ethyl ester in 40 ccs of ethanol is heated to the boil overnight and evaporated in vacuo. Yellow-brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946028 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-9e56f91eb66b4d36836fc145d44140f6 |
| Source note | uspto-grants-1976_03 |