HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → N-(1,3-dioxolan-5-ylmethyl)-2-ethyl-4-chloroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-2-ethylaniline | HCID 34871 | — |
| Reactant | 4-(Chloromethyl)-1,3-dioxolane | HCID 240153 | — |
| Catalyst | Tetraethylammonium Chloride | HCID 5946 | — |
| Product | N-(1,3-dioxolan-5-ylmethyl)-2-ethyl-4-chloroaniline | HCID 21447796 | — |
Reaction Steps
2-Ethyl-4-chloroaniline (0.3 mole), 5-chloromethyl-1,3-dioxolane (0.3 mole), potassium carbonate (0.3 mole) and tetraethylammonium chloride (2 grams) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux for a period of 6 hours. After this time the mixture is filtered and distilled to yield the desired product N-(1,3-dioxolan-5-ylmethyl)-2-ethyl-4-chloroaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946045 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-e27d8900befe4daa99d9fe551509407e |
| Source note | uspto-grants-1976_03 |