HRID268063

反应详情

EQUATION

反应方程式

HRID 268063 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Upon boiling a solution of 2.8 g of acetaldehyde, 5.6 g of cyclohexane-1,3-dione and 6.5 g of amidinoacetic acid ethyl ester in 100 ml of ethanol for 2 hours, 2-amino-4-methyl-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3carboxylic acid ethyl ester of melting point 236°C (ethanol) is obtained.

WORKUP

后处理

  1. customfor 2 hours