HRID268064

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7449

3-Nitrobenzaldehyde

C7H5NO3

HCID10434

1,3-Cyclohexanedione

C6H8O2

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC2=C(C(=O)CCC2)C1c1cccc([N+](=O)[O-])c1

HCID12391117

未命名化合物

收率 61%

PROCEDURE

实验过程

Upon boiling a solution of 7.6 g of 3-nitrobenzaldehyde, 5.6 g of cyclohexane-1,3-dione and 6.5 g of amidinoacetic acid ethyl ester for 1 hour, 2-amino-4-(3-nitrophenyl)-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3-carboxylic acid ethyl ester of melting point >260°C is obtained (alcohol/DMF).

WORKUP

后处理

customfor 1 hour