HRID268065

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10434

1,3-Cyclohexanedione

C6H8O2

HCID11477

Benzaldehyde, 3-chloro-

C7H5ClO

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

HCID19794673

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC2=C(C(=O)CCC2)C1c1cccc(Cl)c1

HCID12391108

未命名化合物

收率 66%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Upon boiling a solution of 7.1 g of 3-chlorobenzaldehyde, 5.6 g of cyclohexane-1,3-dione and 6.5 g of amidinoacetic acid ethyl ester in 150 ml of ethanol for 2 hours, 2-amino-4-(3-chlorophenyl)-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3-carboxylic acid ethyl ester of melting point 266°C (ethanol/DMF) is obtained.

WORKUP

后处理

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