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HRID268081

反应详情

EQUATION

反应方程式

HRID 268081 的结构方程式

REACTANTS

反应物

3
结构：O=C1CCCC(=O)C1
HCID10434

1,3-Cyclohexanedione

C6H8O2

结构：CCOC(=O)CC(=N)N
HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

结构：CCOC(=O)c1cccc(C=O)c1
HCID11084437

Ethyl 3-formylbenzoate

C10H10O3

PRODUCTS

生成物

1
结构：CCOC(=O)C1=C(N)NC2=C(C(=O)CCC2)C1c1cccc(C(=O)OCC)c1
HCID12391116

未命名化合物

收率 54%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Upon heating a solution of 8.9 g of 3-carbethoxybenzaldehyde, 5.6 g of cyclohexane-1,3-dione and 6.5 g of amidinoacetic acid ethyl ester in 100 ml of ethanol for 4 hours, 2-amino-4-(3-carbethoxyphenyl)-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3-carboxylic acid ethyl ester of melting point 234°C (ethanol) is obtained.