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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 268082Generated: November 1, 2026

1,3-Cyclohexanedione → HCID 86733067, compound

https://huagongshe.com/reaction/268082

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-CyclohexanedioneHCID 10434—
ReactantCarbamimidoyl-acetic acid ethyl esterHCID 4599837—
Reactant2-azidobenzaldehydeHCID 10888060—
SolventEthanolHCID 702—
ProductHCID 86733067HCID 8673306758%

Reaction Steps

Upon heating a solution of 7.4 g of 2-azidobenzaldehyde, 5.6 g of cyclohexane-1,3-dione and 6.5 g of amidinoacetic acid ethyl ester in 100 ml of ethanol for 4 hours, 2-amino-4-(2-azidophenyl)-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3-carboxylic acid ethyl ester of melting point 209°C (ethanol) is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03946026
Source datasetuspto-grants-1976_03
ORD IDord-d54833630006446391b940490ecd3179
Source noteuspto-grants-1976_03