HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 53911753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 2-Furancarbonitrile, 5-phenyl- | HCID 12227148 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53911753 | HCID 53911753 | — |
Reaction Steps
A mixture of 10 g (0.059 mole) of 5-phenyl-2-furonitrile, 4.1 g (0.060 mole) of hydroxylamine hydrochloride, 4.0 g (0.060 mole) of potassium hydroxide, and 150 ml of absolute ethanol was refluxed for 21/2 hours, cooled to room temperature, and then added to 750 ml of ice/H2O. the resulting solid was washed in water and dried at 60° to yield 10 g (84%), m.p. 118°-120°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946049 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-7beaed5a0645411fbe62c029073ae1af |
| Source note | uspto-grants-1976_03 |