HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 85436872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 5-(4-methoxyphenyl)furan-2-carbaldehyde | HCID 2759655 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 85436872 | HCID 85436872 | — |
Reaction Steps
A 250 ml Erlenmeyer flask was charged with 5-(4-methoxyphenyl)-2-furaldehyde (40 g, 0.20 mole) and absolute alcohol (125 ml). A solution of hydroxylamine hydrochloride (14 g, 0.20 mole) in water (25 ml) was added to this suspension. This mixture was stirred for 1 hour, cooled, filtered and washed with isopropanol, yielding 28 g (65.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03946049 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-18d19c5b3d264278a56a40064d5153a5 |
| Source note | uspto-grants-1976_03 |