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HRID268120

反应详情

EQUATION

反应方程式

HRID 268120 的结构方程式

REACTANTS

反应物

2
结构：CCCCCc1cc(O)cc(O)c1
HCID10377

Olivetol

C11H16O2

结构：CCOC(=O)C1SC(C)(C)CC1=O
HCID12716257

Ethyl 5,5-dimethyl-3-oxothiolane-2-carboxylate

C9H14O3S

PRODUCTS

生成物

1
结构：CCCCCc1cc(O)c2c3c(c(=O)oc2c1)SC(C)(C)C3
HCID21553565

未命名化合物

收率 72.5%

PROCEDURE

实验过程

Ethyl 5,5-dimethyl-3-oxo-tetrahydrothiophene-2-carboxylate was reacted with 5-n-pentyl resorcinol following a procedure similar to that of Example 3-C to produce 1,2-dihydro-2,2-dimethyl-9-hydroxy-7-n-pentyl-4-oxo-4H-thieno-[2,3-c][1] benzopyran in a 72.5% yield, m.p. 203°-206°C.