Cyanuric chloride → 2,2'-((4,6-Dichloro-1,3,5-triazin-2-yl)imino)bisethanol

Participants

Reaction Conditions

Reaction Steps

25 Grams cyanuric chloride was dissolved in 145 ml. acetone and the solution poured over 100 grams of ice. Sodium bicarbonate (12.4 grams) was added. While maintaining the temperature at 10°C., diethanolamine (15.5 grams) was added dropwise over a period of about 30 minutes. The temperature was raised to 20°-25°C. and the mixture stirred for about 1 hour. The reaction mixture was filtered, washed witth water and dried to give 31.4 grams of product.

Provenance & Evidence