HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 54525598, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | HCID 21030685 | HCID 21030685 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54525598 | HCID 54525598 | — |
Reaction Steps
If 7-chloro-1,2,3,11a-tetrahydro-10-methyl-5 H-pyrrolo[2,1-c] [1,4] benzodiazepin-5,11(10H)-dione (prepared as described in Example 1 from DL-proline and 5 -chloro-N-methylisatoic anhydride) is treated with 1M borane in tetrahydrofuran as described in Example 1, the above compound is obtained. The hydrochloride salt melts at 243°-245°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947408 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-d2a288af25a54d85b7fa4a3779b74cda |
| Source note | uspto-grants-1976_03 |