Borane → HCID 68144896, compound

HRID 268170Notes

Reaction equation

HRID 268170 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([Cl:19])[C:5]2[N:11]([CH3:12])[C:10](=[O:13])[CH:9]3[CH2:14][CH2:15][CH2:16][N:8]3[C:7](=O)[C:6]=2[CH:18]=1.B>>[Cl:1][C:2]1[CH:3]=[C:4]([Cl:19])[C:5]2[N:11]([CH3:12])[C:10](=[O:13])[CH:9]3[CH2:14][CH2:15][CH2:16][N:8]3[CH2:7][C:6]=2[CH:18]=1

Participants

3

Reactant 2

HCID 6331BoraneHCID 68146050HCID 68146050, compound

Product 1

HCID 68144896HCID 68144896, compound

Procedure

If 7,9-dichloro-1,2,3,11a-tetrahydro-10-methyl-5 H-pyrrolo[2,1-c] [1,4] benzodiazepin-5,11(10H)-dione (prepared by reaction of proline and 3,5-dichloro-N-methylisatoic anhydride as described in Example 1) is treated with borane as described in Example 1, the above compound is obtained.

Workup

  1. customthe above compound is obtained

Sources & evidence

ORD record
ord-d4be4ffddc8b4ae1a307aa7fedd0728d
Source dataset
uspto-grants-1976_03
Patent number
US03947408

Reaction notes

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