HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromoaniline → N-(4-bromophenyl)-7-methyl-3H-imidazo[4,5-f]quinolin-9-amine;hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | HCID 178428198 | HCID 178428198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(4-bromophenyl)-7-methyl-3H-imidazo[4,5-f]quinolin-9-amine;hydrochloride | HCID 178428196 | — |
Reaction Steps
A mixture of 37.9 g. (0.174 m.) of the compound of Example I, C., 30 g. (0.174 ml.) of p-bromoaniline and 500 ml. of ethanol was stirred and refluxed overnight. After concentrating in vacuo the residue was recrystallized from 500 m. of MeOH to give 55 g. m.p. 347°-349° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947434 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-cb5d75acd05842f8b313ecb06aa79be6 |
| Source note | uspto-grants-1976_03 |