4-Ethoxyaniline → HCID 178466723, compound

Participants

Reaction Steps

A mixture of 33 g. (0.15 mole) of the compound of Example I, C. and 23 g. (0.15 mole) of p-phenetidine in 1800 ml. of ethanol was refluxed for 6 hr. The solvent was removed by evaporation in vacuo and the residue was slurried with ether. The crude solid was collected by filtration and was recrystallized from ethanol. The product was collected as yellow needles melting at 229°-230° in a yield of 19 g. (36%). Recrystallization from ethanol raised the melting point to 330°-331°.

Provenance & Evidence