HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → HCID 178492119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | HCID 178426076 | HCID 178426076 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178492119 | HCID 178492119 | — |
Reaction Steps
A mixture of 18.5 g. (0.08 m.) of 9-chloro-2,7-dimethylimidazo [4,5-f]-quinoline, 9.85 g. (0.08 m.) of p-anisidine and 300 ml. of ethanol was refluxed, with stirring, overnight. The solution was concentrated in vacuo to give 27 g. m.p. 307°-311°C. Recrystallization from 300 ml. of MeOH yielded 13 g. m.p. 317°-318°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947434 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-98bf7a5ee85d4dd689b8556f128ed564 |
| Source note | uspto-grants-1976_03 |