HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-[4-(3-Diethylaminopropoxy)benzoyl]-2-phenylbenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Chloropropyl(diethyl)amine | HCID 66918 | — |
| Reactant | (4-Hydroxyphenyl)(2-phenyl-1-benzofuran-3-yl)methanone | HCID 13264991 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-[4-(3-Diethylaminopropoxy)benzoyl]-2-phenylbenzofuran | HCID 21435324 | — |
Reaction Steps
A mixture of 6.2 g. (19.7 mmol.) of 3-(4-hydroxybenzoyl)-2-phenylbenzofuran, 2.95 g. (19.7 mmol.) of 3-diethylaminopropyl chloride and 10.9 g. (0.079 mol.) of potassium carbonate in 300 ml. of acetone is refluxed for 12 hours. After cooling, the mixture is filtered and the filtrate is concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947470 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-21a6236886e0486aa90d683e2b7bb6ab |
| Source note | uspto-grants-1976_03 |