HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromopropane → 5-Chloro-3-[4-(3-bromopropoxy)benzoyl]-2-phenylbenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Chloro-3-(4-hydroxybenzoyl)-2-phenylbenzofuran | HCID 21435336 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 5-Chloro-3-[4-(3-bromopropoxy)benzoyl]-2-phenylbenzofuran | HCID 21435390 | — |
Reaction Steps
A mixture of 3.2 g. (9.2 mmol.) of 5-chloro-3-(4-hydroxybenzoyl)-2-phenylbenzofuran, 3.5 ml. (0.035mol.) of 1,3-dibromopropane and 4.0 g. (0.029 mol.) of potassium carbonate in 100 ml. of acetone is refluxed for 3 hours. After cooling, the reaction mixture is filtered and the filtrate is concentrated to give 5-chloro-3-[4-(3-bromopropoxy)benzoyl]-2-phenylbenzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947470 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-db33dc7f1ab64a97a8972b2193b3c737 |
| Source note | uspto-grants-1976_03 |