HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 1-(4-chlorophenyl)-2-phenoxyethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-(4-chlorophenyl)-2-phenoxyethanone | HCID 1471526 | — |
Reaction Steps
A mixture of 23.3 g. (0.1 mol.) of α-bromo-p-chloroacetophenone, 10.0 g. (0.1 mol.) of phenol and 14.5 g. (0.1 mol.) of potassium carbonate in 65 ml. of dry acetone is refluxed for 12 hours. The reaction mixture is cooled, poured into 500 ml. of water and the precipitate formed is collected by filtration and recrystallized from ethanol to give α-phenoxy-p-chloroacetophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947470 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-3468924a76934c5aba7efca96c45cd83 |
| Source note | uspto-grants-1976_03 |