HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → 2-[4-(1-Bromoethyl)phenyl]benzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 2-(4-Ethyl-phenyl)-benzooxazole | HCID 3993383 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 2-[4-(1-Bromoethyl)phenyl]benzoxazole | HCID 23459165 | — |
Reaction Steps
To a solution of 7.1 gm. of 2-(4-ethylphenyl) benzoxazole in 125 cc. of carbon tetrachloride is added 6.2 gm. of N-bromosuccinimide and 50 mg. of benzoyl peroxide. The mixture is refluxed for about one half hour at which time the N-bromosuccinimide was consumed. Filtration followed by concentration of the filtrate gives 2-(4-[1-bromoethyl]phenyl)benzoxazole, m.p. 128°-131°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947582 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-3aafaef2dd9b423588de63ceee196fc0 |
| Source note | uspto-grants-1976_03 |