HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-(3-Amino-3-oxoprop-1-en-2-yl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21413842 | HCID 21413842 | — |
| Product | 4-(3-Amino-3-oxoprop-1-en-2-yl)benzoyl chloride | HCID 21413822 | — |
Reaction Steps
A mixture of 50 cc. of thionyl chloride and 0.05 moles of p-carboxyatropamide is heated at reflux on the steam-bath for 1/2 hour. The reaction mixture is concentrated in vacuo to give p-chlorocarbonylatropamide suitable for use in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03947582 |
| Source dataset | uspto-grants-1976_03 |
| ORD ID | ord-f2c810ecf6614f0890a0fcb34e724931 |
| Source note | uspto-grants-1976_03 |