HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-9H-fluorene → 2-Acetyl-7-bromofluorene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-9H-fluorene | HCID 14336 | — |
| Reactant | acetic anhydride AlCl3 nitrobenzene | HCID 86587524 | — |
| Product | 2-Acetyl-7-bromofluorene | HCID 270675 | — |
Reaction Steps
1-(7-bromo-9H-fluoren-2-yl)-ethanone is prepared by the reaction of 2-bromofluorene (available from Aldrich Chemical Company, Milwaukee, Wis.) with acetic anhydride/AlCl3/nitrobenzene according to Tsuno et al., Bull. Chem. Soc. Jpn., 51, 601-607 (1978), incorporated herein by reference.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07445825B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-3be9e6a1ff784fccb293c9e66a4165de |
| Source note | uspto-grants-2008_11 |