HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 5-Bromo-2,4-difluoro-N-(2-hydroxyethyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 5-Bromo-2,4-difluorobenzenesulphonyl chloride | HCID 2773296 | — |
| Product | 5-Bromo-2,4-difluoro-N-(2-hydroxyethyl)benzenesulfonamide | HCID 67000352 | 100% |
Reaction Steps
Prepared by general procedure III from 5-bromo-2,4-difluorobenzene sulfonyl chloride (1.0 g, 3.4 mmol) and ethanolamine (231 mg, 3.77 mmol) to give the title compound (1.06 g, 100%) as an off-white solid. MS (ISP) 315.8[(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446113B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-2fc06ae03a784eb6b796ba4e6cdd4f89 |
| Source note | uspto-grants-2008_11 |