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HRID269142

反应详情

EQUATION

反应方程式

HRID 269142 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1cncc(Br)c1
HCID12684258

5-Bromopyridine-3-sulfonamide

C5H5BrN2O2S

结构：C#Cc1cnn2c(C3CC3)cc(-c3ccc(Cl)cc3)nc12
HCID86607996

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1cncc(C#Cc2cnn3c(C4CC4)cc(-c4ccc(Cl)cc4)nc23)c1
HCID67000987

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-(4-chloro-phenyl)-7-cyclopropyl-3-ethynyl-pyrazolo[1,5-a]pyrimidine (example C.5) (147 mg, 0.5 mmol) and 5-bromo-pyridine-3-sulfonic acid amide (119 mg, 0.5 mmol) according to general procedure II. Obtained as a yellow solid (177 mg, 79%). MS (ISP) 449.9 [(M+H)+]; mp 252-254° C.