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HRID269146

反应详情

EQUATION

反应方程式

HRID 269146 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1cc(Br)c(F)cc1F
HCID2773295

5-bromo-2,4-difluorobenzenesulfonamide

C6H4BrF2NO2S

结构：C#Cc1cnn2c(C3CC3)cc(-c3ccc(Cl)cc3)nc12
HCID86607996

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1cc(C#Cc2cnn3c(C4CC4)cc(-c4ccc(Cl)cc4)nc23)c(F)cc1F
HCID67001101

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-(4-chloro-phenyl)-7-cyclopropyl-3-ethynyl-pyrazolo[1,5-a]pyrimidine (example C.5) (73 mg, 0.25 mmol) and 5-bromo-2,4-difluoro-benzenesulfonamide (68 mg, 0.25 mmol) according to general procedure II. Obtained as a yellow solid (91 mg, 75%). MS (ISP) 485.1 [(M+H)+]; mp 272-275° C.