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HRID269162

反应详情

EQUATION

反应方程式

HRID 269162 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1ccc(Br)s1
HCID1241304

5-Bromothiophene-2-sulfonamide

C4H4BrNO2S2

结构：C#Cc1cnn2c(C3CC3)cc(-c3ccc(Cl)c(Cl)c3)nc12
HCID86608050

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1ccc(C#Cc2cnn3c(C4CC4)cc(-c4ccc(Cl)c(Cl)c4)nc23)s1
HCID67000720

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 7-cyclopropyl-5-(3,4-dichloro-phenyl)-3-ethynyl-pyrazolo[1,5-a]pyrimidine (Example C.8) (82 mg, 0.25 mmol) and 5-bromo-thiophene-2-sulfonic acid amide (61 mg, 0.25 mmol) according to general procedure II. Obtained as a yellow solid (35 mg, 28%). MS (ISP) 489.3 [(M+H)+]; mp 213-214° C.