huagongshe.com
HRID269170

反应详情

EQUATION

反应方程式

HRID 269170 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(CO)NS(=O)(=O)c1cccc(Br)c1
HCID43501900

未命名化合物

结构：C#Cc1cnn2c(C(F)(F)F)cc(-c3ccc(Cl)cc3)nc12
HCID86607995

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(CO)NS(=O)(=O)c1cccc(C#Cc2cnn3c(C(F)(F)F)cc(-c4ccc(Cl)cc4)nc23)c1
HCID67000257

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-(4-chloro-phenyl)-3-ethynyl-7-trifluoromethyl pyrazolo[1,5-a]pyrimidine (example C.4) (322 mg, 1.0 mmol) and 3-bromo-N-(2-hydroxy-1,1-dimethyl-ethyl)-benzenesulfonamide (370 mg, 1.2 mmol) according to general procedure II. Obtained as a yellow solid (244 mg, 44%). MS (ISP) 549.3 [(M+H)+]; mp 226-229° C.