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HRID269224

反应详情

EQUATION

反应方程式

HRID 269224 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1ccc(Br)s1
HCID1241304

5-Bromothiophene-2-sulfonamide

C4H4BrNO2S2

结构：C#Cc1cnn2c(C(C)(C)O)cc(-c3ccc(Cl)cc3)nc12
HCID86608078

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1ccc(C#Cc2cnn3c(CO)cc(-c4ccc(Cl)cc4)nc23)s1
HCID67001034

未命名化合物

PROCEDURE

实验过程

The title compound was prepared 2-[5-(4-chloro-phenyl)-3-ethynyl-pyrazolo[1,5-a]pyrimidin-7-yl]-propan-2-ol (example C.14) (28 mg, 0.1 mmol) and 5-bromo-thiophene-2-sulfonic acid amide (24 mg, 0.10 mmol) according to general procedure II. Obtained as a yellow solid (9 mg, 20%). MS (ISP) 445.0 [(M+H)+]; mp 194-196° C.