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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 269340Generated: October 31, 2026

HCID 67000954, compound → HCID 86608122, compound

https://huagongshe.com/reaction/269340

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67000954HCID 67000954—
Reactant3-Ethynyl-7-trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidineHCID 71539732—
ProductHCID 86608122HCID 86608122—

Reaction Steps

The title compound was prepared from 3-ethynyl-7-trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine (example C.1) (178 mg, 0.5 mmol) and 5-bromo-thiophene-2-sulfonic acid (2,6-dimethyl-pyridin-4-ylmethyl)-amide (example B.58) (181 mg, 0.5 mmol) according to general procedure II. Obtained as an orange solid (120 mg, 38%). MS (ISN) 634.0 [(M−H)−]; mp 200° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07446113B2
Source datasetuspto-grants-2008_11
ORD IDord-e30cc02f3f614beca353d51d277fe67f
Source noteuspto-grants-2008_11