Phenylboronic Acid → HCID 68959602, compound

Participants

Reaction Steps

The title compound was prepared as a solid (0.202 g, 68%) by the coupling of 5-(3-bromo-1-benzofuran-2-yl)-8-methoxy-quinoline and phenyl boronic acid according to the procedure described in Step 1 of Example 1. Mass spectrum (+ESI, [M+H]+) m/z 352. 1H NMR (400 MHz, DMSO-d6): δ 8.87 (d, 1H, J=1.6 Hz), 8.13 (d, 1H, J=8.2 Hz), 7.73 (t, 2H, J=7.8 Hz), 7.68 (d, 1H, J=8.2 Hz), 7.38-7.52 (m, 3H), 7.21-7.38 (m, 6H), and 4.00 ppm (s, 3H).

Provenance & Evidence