HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57440193, compound → tert-Butyl {(3S)-4-amino-3-[(tert-butoxycarbonyl)amino]butyl}carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57440193 | HCID 57440193 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | tert-Butyl {(3S)-4-amino-3-[(tert-butoxycarbonyl)amino]butyl}carbamate | HCID 57440194 | — |
Reaction Steps
Preparation takes place in analogy to Example 86A from 171 mg (0.52 mmol) of tert-butyl{(3S)-4-azido-3-[(tert-butoxycarbonyl)amino]butyl}carbamate (Example 91A) in 10 ml of ethanol with the addition of 20 mg of palladium on activated carbon (10%). The product is reacted without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07446102B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-96eaa377cfe14e8fbcce41788b1fd7dd |
| Source note | uspto-grants-2008_11 |