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HRID269621

反应详情

EQUATION

反应方程式

HRID 269621 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)NCC[C@@H](CO)NC(=O)[C@H](CCCNC(=O)OCc1ccccc1)NC(=O)OC(C)(C)C
HCID131727148

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCC[C@@H](CO)NC(=O)[C@H](CCCN)NC(=O)OC(C)(C)C
HCID86619424

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Preparation takes place in analogy to Example 81A from 50 mg (0.09 mmol) of benzyl((4S)-4-[(tert-butoxycarbonyl)amino]-5-{[(1S)-3-[(tert-butoxycarbonyl)amino]-1-(hydroxymethyl)propyl]amino}-5-oxopentyl)carbamate (Example 93A) in 50 ml of ethanol with the addition of 5 mg of palladium on activated carbon (10%). The product is reacted without further purification.

WORKUP

后处理

  1. customPreparation
  2. customThe product is reacted without further purification