HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methyl]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 20394050 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methyl]benzeneethanamine | HCID 21322756 | 74.9% |
Reaction Steps
N-[[2-[3-(4-Morpholinyl)propoxy]phenyl]methylene]-benzeneethanamine (17 g) is reduced with 5.4 g of sodium borohydride in 85 ml of methanol following the procedure described in Example 1B to yield 12.8 g of product as an oil, boiling point 219°-223° C. at 0.1-0.2 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151354 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-d216ba75c7b541d9a27f8475fc2f95a6 |
| Source note | uspto-grants-1979_04 |