HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 2-(2-Morpholinoethoxy)benzaldehyde | HCID 976593 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine | HCID 21322775 | 85.6% |
Reaction Steps
2-[2-(4-Morpholinyl)ethoxy]benzaldehyde (55.9 g) is reacted with 29 g of phenethylamine in 240 ml of toluene following the procedure described in Example 1A to yield 68.8 g of product as an oil, boiling point 204°-210° C. at 0.1-0.2 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151354 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-4ac30af58cde4ba28f2ed7a5aea79b00 |
| Source note | uspto-grants-1979_04 |