HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-[[2-[3-(1-Piperidinyl)propoxy]phenyl]methylene]benzeneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 2-[3-(1-Piperidinyl)propoxy]benzaldehyde | HCID 13795259 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[[2-[3-(1-Piperidinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 21322776 | 91.8% |
Reaction Steps
2-[3-(1-Piperidinyl)propoxy]benzaldehyde (47.6 g) is reacted with 24 g of phenethylamine in 190 ml of toluene following the procedure described in Example 1A to yield 61.9 g of product as an oil, boiling point 214°-218° C. at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151354 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-77589dc074c64d02b6d2d37be4ed4702 |
| Source note | uspto-grants-1979_04 |