HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium borohydride → N-[[2-[3-(1-Piperidinyl)propoxy]phenyl]methyl]benzeneethanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium borohydride | HCID 4311764 | — |
| Edukt | N-[[2-[3-(1-Piperidinyl)propoxy]phenyl]methylene]benzeneethanamine | HCID 21322776 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | N-[[2-[3-(1-Piperidinyl)propoxy]phenyl]methyl]benzeneethanamine | HCID 21322750 | 80,2% |
Reaktionsschritte
N-[[2-[3-(1-Piperidinyl)propoxy]phenyl]methylene]benzeneethanamine (61.5 g) is reduced with 20 g of sodium borohydride in 320 ml of methanol following the procedure described in Example 1B to yield 49.6 g of product as an oil, boiling point 216°-221° C. at 0.3-0.4 mm of Hg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04151354 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-e78b74366ff64dd194c19aa1528eb770 |
| Quellennotiz | uspto-grants-1979_04 |