HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → (Z,E)-N,N-diethyl-8-hydroxy-3,7-dimethyl-2,6-octadienamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | (Z,E)-8-hydroxy-3,7-dimethyl-2,6-octadienoic acid | HCID 12681379 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (Z,E)-N,N-diethyl-8-hydroxy-3,7-dimethyl-2,6-octadienamide | HCID 86736490 | — |
Reaction Steps
Following the same manner as in Example 5, the reaction and after-treatment were conducted by using 1.0 g of (E,E) and (Z,E)-8-hydroxy-3,7-dimethyl-2,6-octadienoic acid, 0.9 ml of triethylamine, 0.62 ml of ethyl chlorocarbonate and 0.67 ml of diethylamine in 20 ml of dichloromethane to afford 850 mg of the end product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151357 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-e5718d830887400eb311942a357d5ece |
| Source note | uspto-grants-1979_04 |