HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 59833604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 11327963 | HCID 11327963 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 59833604 | HCID 59833604 | 72.3% |
Reaction Steps
A solution of 0.5 g (1.15 mmol) of sulfone 1 and 0.11 g (1.62 mmol) of sodium azide in acetonitrile was refluxed for 2 hours. Cooling, distillative removal of the solvent and digestion of the residue with water gave 0.33 g of the title compound of m.p. 152-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449471B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-d4a3ece1b01d4bbf9b9b7bfaad80d684 |
| Source note | uspto-grants-2008_11 |