HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Cyanide → HCID 59833602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | HCID 86606165 | HCID 86606165 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 59833602 | HCID 59833602 | 71.3% |
Reaction Steps
A solution of 1.0 g (2.63 mmol) of sulfone 3 and 0.21 g (3.16 mmol) of potassium cyanide in acetonitrile was stirred at 20-25° C. for 5 days. The solvent was distilled off and the residue was digested with MTBE:ethyl acetate [EA] 9:1. Filtration and concentration of the filtrate gave 0.61 g of the title compound of m.p 186-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07449471B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-4ba35c1b04574eef9d4f13c4e433ef05 |
| Source note | uspto-grants-2008_11 |