HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium 2-ethylhexanoate → (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-1-ol disulfate sodium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium 2-ethylhexanoate | HCID 23672331 | — |
| Reactant | (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-ol disulfate pyridine salt | HCID 86736496 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-1-ol disulfate sodium salt | HCID 86736497 | — |
Reaction Steps
Following the procedures of Example 27, a solution of 2.2 g of (E,Z,E) and (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-1-ol disulfate pyridine salt prepared in Example 28 in 20 ml of ethyl acetate was treated with 6.0 ml (2 mM/ml) of sodium 2-ethylhexanoate to afford 1.4 g of the end product as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04151357 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-06952ef84f1d496297d27c718088870f |
| Source note | uspto-grants-1979_04 |