huagongshe.com
HRID269948

反应详情

EQUATION

反应方程式

HRID 269948 的结构方程式

REACTANTS

反应物

4
结构：CC(C)CC(=O)Cl
HCID66054

Butanoyl chloride, 3-methyl-

C5H9ClO

结构：O=S(=O)(Cl)Cc1ccc(Cl)cc1
HCID227304

(4-Chlorophenyl)methanesulfonyl chloride

C7H6Cl2O2S

结构：COc1ccc(N2CCNCC2)cc1.Cl.Cl
HCID2723700

1-(4-Methoxyphenyl)-piperazine, dihydrochloride

C11H18Cl2N2O

结构：COc1cc(F)c(N2CCNCC2)cc1F
HCID23111492

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(F)c(N2CCN(S(=O)(=O)Cc3ccc(Cl)cc3)CC2)cc1F
HCID23111489

未命名化合物

收率 100.6%

PROCEDURE

实验过程

Production Example 3 was repeated except that 1-(4-methoxyphenyl)piperazine dihydrochloride and isovaleryl chloride were replaced with 1-(2,5-difluoro-4-methoxyphenyl)-piperazine (228 mg) and 4-chlorobenzylsulfonyl chloride (338 mg), respectively, to provide crude 1-(4-chlorobenzylsulfonyl)-4-(2,5-difluoro-4-methoxyphenyl)piperazine (419 mg).