N-(2-Methoxyethyl)ethylamine → HCID 22314195, compound

HRID 270381Notes

Reaction equation

HRID 270381 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:12]3[CH:13]=[CH:14][C:15]([CH2:17][CH2:18][CH2:19][CH2:20]OS(C)(=O)=O)=[CH:16][C:11]=3[S:10][N:9]=2)=[CH:4][CH:3]=1.[CH3:26][O:27][CH2:28][CH2:29][NH:30][CH2:31][CH3:32]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:12]3[CH:13]=[CH:14][C:15]([CH2:17][CH2:18][CH2:19][CH2:20][N:30]([CH2:31][CH3:32])[CH2:29][CH2:28][O:27][CH3:26])=[CH:16][C:11]=3[S:10][N:9]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 546877N-(2-Methoxyethyl)ethylamineHCID 57428084Methanesulfonic acid 4-[3-(4-chloro-phenyl)-benzo[d]isothiazol-6-yl]-butyl ester

Product 1

HCID 22314195HCID 22314195, compound

Procedure

According to the method in example 23, Methanesulfonic acid 4-[3-(4-chloro-phenyl)-benzo[d]isothiazol-6-yl]-butyl ester and N-(2-Methoxyethyl)ethylamine were converted to yield {4-[3-(4-Chloro-phenyl)-benzo[d]isothiazol-6-yl]-butyl}-ethyl-(2-methoxy-ethyl)-amine, MS: 403 (MH+, 1Cl).

Sources & evidence

ORD record
ord-72e8558fc9bb433a86297e298bf233cd
Source dataset
uspto-grants-2008_11
Patent number
US07449483B2

Reaction notes

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